Влияние когерентной двойниковой границы на высокотемпературную ползучесть стали 321SS (12Х18Н10Т), не стабилизированной титаном
Аннотация
Для исследования использовали коммерческие пластины из нержавеющей стали 321 (12Х18Н10Т), которые подвергались обработке методом инженерии границ зерен (ИГЗ). Обнаружено, что доля длины границ решетки с низким значением Σ узлов совпадения (Σ3 + Σ9 + Σ27) увеличилась с 39,3 % (до обработки ИГЗ) до 75,9 % (после обработки ИГЗ), а доля когерентных границ Σ3 увеличилась с 26,2 % до 58,1 %. Испытания на ползучесть проводили при 550 °C под действием различных напряжений на образцах стали, не стабилизированной титаном. Результаты показали, что сопротивление высокотемпературной ползучести стали возрастает более чем на 70 % после обработки ИГЗ. Анализ методом дифракции обратного рассеяния электронов и наноиндентирования показал, что концентрация напряжений ползучести на когерентных двойниковых границах (КДГ) ниже, чем на случайных границах зерен, что снижает вероятность образования пустот или трещин на КДГ. Кроме того, КДГ оказывают подавляющее действие на распространение трещин на границах зерен. Результаты этого исследования имеют важное значение для углубления понимания роли КДГ в высокотемпературной деформации ползучести металлических материалов c ГЦК-решеткой без вторичных фаз в структуре.
Ключевые слова
Литература
Reddy G P, Dinesh P, Sandhya R, et al. Jayakumar T. Behavior of 321 stainless steel under engineering stress and strain controlled fatigue // International Journal of Fatigue, 2016, 92: 272-280.
Hu Y, Bai Q, Xia S, et al. Applying grain boundary engineering and stabilizing heat treatment to 321 stainless steel for enhancing intergranular corrosion resistance // Journal of Materials Engineering and Performance, 2024,33(16): 8202-8213.
Swindeman R, Farrell K, Yoo M. Intergranular microcavities in type 304 stainless steel // Research in Mechanica Letters, 1981, 1(2): 67-71.
Arzate O, Martinez L. Creep cavitation in type 321 stainless steel // Materials Science and Engineering: A, 1988, 101: 1-6.
Petkov M P, Elmukashfi E, Cocks A C. Multi-scale modelling of creep cavity nucleation and growth in polycrystalline type 316 stainless steel // Philosophical Magazine, 2022, 102(23): 2362-2411.
Goodhew P. Annealing twin formation by boundary dissociation // Metal Science, 1979, 13(3-4): 108-112.
Priester L. Geometrical speciality and special properties of grain boundaries // Revue de Physique Appliquée, 1989, 24(4): 419-438.
Kokawa H, Watanabe T, Karashima S. Sliding behaviour and dislocation structures in aluminium grain boundaries // Philosophical Magazine A, 1981, 44(6): 1239-1254.
Don J, Majumdar S. Creep cavitation and grain boundary structure in type 304 stainless steel // Acta Metallurgica, 1986, 34(5): 961-967.
He J, Sandström R. Formation of creep cavities in austenitic stainless steels // Journal of Materials Science, 2016, 51: 6674-6685.
Watanabe T. An approach to grain boundary design for strong and ductile polycrystals // Res Mechanica, 1984, 11(1): 47-84.
Shimada M, Kokawa H, Wang Z, et al. Optimization of grain boundary character distribution for intergranular corrosion resistant 304 stainless steel by twin-induced grain boundary engineering // Acta Materialia, 2002, 50(9): 2331-2341.
Xia S, Zhou B, Chen W, et al. Effects of strain and annealing processes on the distribution of Σ3 boundaries in a Ni-based superalloy // Scripta Materialia, 2006, 54(12): 2019-2022.
Randle V. The influence of annealing twinning on microstructure evolution // Journal of Materials Science, 2005, 40: 853-859.
Wang W, Zhou B, Rohrer G S, et al. Textures and grain boundary character distributions in a cold rolled and annealed Pb–Ca based alloy // Materials Science and Engineering: A, 2010, 527(16-17): 3695-3706.
Was G S, Thaveeprungsriporn V, Crawford D C. Grain boundary misorientation effects on creep and cracking in Ni-based alloys // JOM, 1998, 50(2): 44-49.
Lehockey E, Palumbo G. On the creep behaviour of grain boundary engineered nickel // Materials Science and Engineering: A, 1997, 237(2): 168-172.
Wang W, Yin F, Guo H, et al. Effects of recovery treatment after large strain on the grain boundary character distributions of subsequently cold rolled and annealed Pb–Ca–Sn–Al alloy // Materials Science and Engineering: A, 2008, 491(1-2): 199-206.
Wang W, Cui Y, Rohrer G S, et al. Grain boundary inter-connections of ∑ 5 boundaries in a high purity iron with a uniform microstructure // Scripta Materialia, 2019, 170: 62-66.
Dunn D, Shiflet G, Hull R. Quantitative three-dimensional reconstruction of geometrically complex structures with nanoscale resolution // Review of Scientific Instruments, 2002, 73(2): 330-334.
Rollett A D, Lee S-B, Campman R, et al. Three-dimensional characterization of microstructure by electron back-scatter diffraction // Annual Review of Materials Research, 2007, 37(1): 627-658.
Du A, Wang W, Gu X, et al. The dependence of precipitate morphology on the grain boundary types in an aged Al–Cu binary alloy // Journal of Materials Science, 2021, 56: 781-791.
Rohrer G S, Saylor D M, El Dasher B, et al. The distribution of internal interfaces in polycrystals // International Journal of Materials Research, 2021, 95(4): 197-214.
Saylor D M, El-Dasher B S, Adams B L, et al. Measuring the five-parameter grain-boundary distribution from observations of planar sections // Metallurgical and Materials Transactions A, 2004, 35: 1981-1989.
Wang W, Dai Y, Li J, et al. An atomic-level mechanism of annealing twinning in copper observed by molecular dynamics simulation // Crystal Growth & Design, 2011, 11(7): 2928-2934.
Wang W, Chen S, Rohrer G S, et al. The inter-connections of ∑ 3 boundaries in pure iron // Scripta Materialia, 2017, 128: 18-22.
Wang W, Du A, Yang X, et al. (2021) Quantitative determination of grain boundary inter-connections // CN Patent No. CN202011173146.8.
Abdeljawad F, Lu P, Argibay N, et al. Grain boundary segregation in immiscible nanocrystalline alloys // Acta Materialia, 2017, 126: 528-539.
Wang W, Cai C, Rohrer G S, et al. Grain boundary inter-connections in polycrystalline aluminum with random orientation // Materials Characterization, 2018, 144: 411-423.
Wright S, Larsen R. Extracting twins from orientation imaging microscopy scan data // Journal of Microscopy, 2002, 205(3): 245-252.
Watanabe T, Davies P W. Grain boundary sliding and intergranular fracture behaviour of copper bicrystals // Philosophical Magazine A, 1978, 37(5): 649-681.
Biscondi M, Goux C. Intercrystalline creep of oriented aluminium bicrystals // Mémoires Scientifiques de la Revue de Métallurgie, 1968, 65(2): 167-179.
Lagarde P, Biscondi M. Fluage intergranulaire de bicristaux symétriques de flexion autour de〈100〉 dans l'aluminium // Canadian Metallurgical Quarterly, 1974, 13(1): 245-251.
Lagarde P, Biscondi M. Intercrystalline creep of orientated Cu bicrystals // Mémoires Scientifiques de la Revue de Métallurgie, 1974, 71(2): 121-131.
Michaut B, Silvent A, Sainfort G. Intergranular creep of stainless steel bicrystals // Memoires Scientifiques de la Revue de Metallurgie, 1974, 71(9): 527-538.
Pond R, Smith D, Southerden P. On the role of grain boundary dislocations in high temperature creep // Philosophical Magazine A, 1978, 37(1): 27-40.
Svensson L-E, Dunlop G. The role of interfacial dislocations in the nucleation of intergranular creep cavities // Canadian Metallurgical Quarterly, 1979, 18(1): 39-47.
Howell P, Jones A, Horsewell A, et al. The creation and accommodation of extrinsic dislocations at grain boundaries // Philosophical Magazine, 1976, 33(1): 21-31.
Clark W, Smith D. Interaction of lattice dislocations with periodic grain boundary structures // Journal of Materials Science, 1979, 14: 776-788.
Kegg G, Horton C, Silcock J. Grain boundary dislocations in aluminium bicrystals after high-temperature deformation // Philosophical Magazine, 1973, 27(5): 1041-1055.
Horton C, Silcock J. Grain boundary dislocations and the mechanism of sliding in symmetrical [011] tilt Al bicrystals // Journal of Microscopy, 1974, 102(3): 339-347.
Howell P, Nilsson J, Dunlop G. The effect of creep deformation on the structure of twin boundaries // Philosophical Magazine A, 1978, 38(1): 39-47.
Perry A. Cavitation in creep // Journal of Materials Science, 1974, 9: 1016-1039.
Raj R, Ashby M. Intergranular fracture at elevated temperature // Acta Metallurgica, 1975, 23(6): 653-666.
Watanabe T. Grain boundary sliding and stress concentration during creep // Metallurgical Transactions A, 1983, 14: 531-545.
Lim L, Raj R. Effect of boundary structure on slip-induced cavitation in polycrystalline nickel // Acta Metallurgica, 1984, 32(8): 1183-1190.
Palumbo G, King P, Aust K, et al. Grain boundary design and control for intergranular stress-corrosion resistance // Scripta Metallurgica et Materialia, 1991, 25(8): 1775-1780.
Weaver C. The influence of annealing twins on intergranular creep cracking // Journal of the Institute of Metals, 1958, 87(4): 126-127.
DOI: https://doi.org/10.30906/mitom.2025.7.5-6
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